Determination of the local structure of a highly dispersed Pd-Nanosystem located on a titanium dioxide carrier

Journal of Surface Investigation-X-Ray Synchrotron and Neutron Techniques, 4 (2010) 636-639

This work is devoted to a structural study of a highly dispersed Pd nanosystem, which is stabilized in the TiO2 matrix, by XAFS spectroscopy. Nanocomposite was prepared from bimetallic PdCo(mu-OOCMe)(4)(NCMe) precursor followed by processing in several ways: calcination in air and in argon and microwave irradiation. The local structure of Pd catalysts formed by different methods was studied. Possible structural models were considered in detail.

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